An Old Story in New Light: X-Ray Powder Diffraction Provides Novel Insights into a Long-Known Organic Solid-State Rearrangement Reaction

Halasz, Ivan and Cindro, Nikola and Dinnebier, Robert E. and Vančik, Hrvoj (2013) An Old Story in New Light: X-Ray Powder Diffraction Provides Novel Insights into a Long-Known Organic Solid-State Rearrangement Reaction. Croatica Chemica Acta, 86 (2). pp. 187-192. ISSN 0011-1643

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Abstract

The first in situ diffraction study of the long-known solid-state rearrangement of p-bromobenzeneazotribenzoylmethane is reported. This proof-of-principle study demonstrates how modern laboratory X-ray powder diffraction, accompanied by up-to-date processing tools, can be used to monitor and describe mechanisms of organic solid-state reactions while it also underpins its necessity for structural characterisation of in situ formed crystalline phases.

Item Type: Article
Keywords: powder diffraction; hot-stage microscopy; solid-state reaction; rearrangement; optical microscopy
Date: 2013
Subjects: NATURAL SCIENCES > Chemistry > Organic Chemistry
Divisions: Faculty of Science > Department of Chemistry
Publisher: Hrvatsko kemijsko društvo
Related URLs:
Depositing User: Branka Maravic
Date Deposited: 24 Apr 2014 14:04
Last Modified: 24 Apr 2014 14:04
URI: http://digre.pmf.unizg.hr/id/eprint/949

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